Dataset: Porous Polymers for Generating Slow Relaxing Hyperpolarization under Benchtop-DNP conditions.

Data.zip is a compressed folder contaning all the NMR data recorded. It is made of 2 subfolder: 77K_1T_DNP-TE_experiments, for Low temperature DNP and thermal equilibrium experiment 298K_1T_experiments, for room temperature relaxation experiments EPR_Data, containg exported text file from the EMXnano instrument and EPR-masses.xslx containing a recap of the mass used and the fitted data MATLAB_scripts.zip is a compressed folder containting all the MATLAB script used to fit the data from Data.zip. It contains: rbnmrQC.m, a function required to import topspin data, DNP_spectra_vf.m, a script used to automaatically determine the optimum of the DNP curve Enhancement_from_vd.m, a script used to compute enhancement based on build-up experiments (1 from DNP, and 1 from TE) Fit_function_vf.m, a script used to fit the build-up experiments A folder called Fit_fucntions, containing the following fitting fuctions called by Fit_function_vf.m Fit_biexp_full.m, to fit a bi-exponential stretched build-up Fit_decay_full.m, to fit a monoexponential decay Fit_single_full.m, to fit a monoexponential build-up Excel-result-recap.xslx is an excel file that recap of all the results computed by the fits, the folder used, experiment fitted and integral regions if needed Sample_1H-13C_content-spin-diffusion.xlsx, is an excel file that contains all the data and calculation used to compute spin diffusion and 1H / 13C content of all samples.Data.zip 为包含所有已记录核磁共振（Nuclear Magnetic Resonance, NMR）数据的压缩文件夹，其内含以下子文件夹： 1. 77K_1T_DNP-TE_experiments：用于低温动态核极化（Dynamic Nuclear Polarization, DNP）与热平衡（Thermal Equilibrium, TE）实验； 2. 298K_1T_experiments：用于室温弛豫实验； 3. EPR_Data：包含从EMXnano电子顺磁共振（Electron Paramagnetic Resonance, EPR）仪器导出的文本文件，以及记录所用试剂质量与拟合数据汇总的EPR-masses.xslx文件。 MATLAB_scripts.zip 为包含所有用于拟合Data.zip中数据的MATLAB脚本的压缩文件夹，其内容如下： - rbnmrQC.m：用于导入TopSpin数据的函数； - DNP_spectra_vf.m：用于自动确定DNP曲线最优值的脚本； - Enhancement_from_vd.m：用于基于累积实验（其中1组来自DNP实验，1组来自TE实验）计算增强因子的脚本； - Fit_function_vf.m：用于拟合累积实验的脚本； - 名为Fit_fucntions的文件夹，内含Fit_function_vf.m调用的以下拟合函数： - Fit_biexp_full.m：用于拟合双指数拉伸累积曲线； - Fit_decay_full.m：用于拟合单指数衰减曲线； - Fit_single_full.m：用于拟合单指数累积曲线。 Excel-result-recap.xslx 为汇总所有拟合计算结果、所用文件夹、拟合实验及所需积分区域的Excel文件； Sample_1H-13C_content-spin-diffusion.xlsx 为包含所有用于计算所有样品的自旋扩散与1H/13C含量的数据及计算过程的Excel文件。