Pt(PEt3)(κ2-P,C-PEt2CHMe)(C6Cl5): An Unexpected Intermediate in the Synthesis of cis-Pt(PEt3)2(Cl)(C6Cl5)
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https://figshare.com/articles/dataset/Pt_PEt_sub_3_sub_sup_2_sup_P_C_PEt_sub_2_sub_CHMe_C_sub_6_sub_Cl_sub_5_sub_An_Unexpected_Intermediate_in_the_Synthesis_of_i_cis_i_Pt_PEt_sub_3_sub_sub_2_sub_Cl_C_sub_6_sub_Cl_sub_5_sub_/2676841
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Addition of 1 to 6 equiv of LiC6Cl5 to cis-Pt(PEt3)2Cl2 gives the unexpected phosphine ligand C−H bond activation product Pt(PEt3)(κ2-P,C-PEt2CHMe)(C6Cl5) (1). Aqueous HCl addition to 1 gives the previously reported product of the reaction, cis-Pt(PEt3)2(Cl)(C6Cl5) (2).
创建时间：
2016-02-23
