Ballari_et_al_Supporting_Information_03_Compounds_Characterization.pdf
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Compounds characterization.
UV-vis characterization of the fluorescent proline analogue 1-NBD, as well as NMR spectral characterization of all final compounds.
Prediction of physicochemical properties of fluorescent analogues was performed using molinspiration platform (http://www.molinspiration.com). UV-visible absorption spectra were obtained using a Shimadzu MultiSpec 1501 UV-vis spectrophotometer. Emision and excitation spectra were obtained using a Varian Cary Eclipse spectroluminometer.
1H and 13C NMR spectra were acquired on a Bruker Avance II 300 MHz (75.13 MHz) using CDCl3 as solvent. Chemical shifts (δ) were reported in ppm downfield from tetramethylsilane and coupling constants are in hertz (Hz). NMR spectra were obtained at 298 K unless otherwise stated and samples run as a dilute solution of the stated solvent. All NMR spectra were referenced to the residual undeuterated solvent as an internal reference.
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RDA UNR
创建时间:
2024-03-05



