wil-190619-180641_oa
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This dataset contains NMR spectra obtained for the sample -wil-190619-180641_oa date: 2019-06-19T16:33:02.000Z isFt: false name: wil-190619-180641_oa/1 phc0: 13.77798 phc1: 48.38174 type: NMR FID DECIM: 3328 aqMod: 3 isFid: true tdOff: 0 title: Parameter file, TOPSPIN Version 3.2 DSPFVS: 20 nucleus: 1H reverse: false solvent: CDCl3 dimension: 1 increment: 0.00008319999999999985 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z828401/0054 experiment: 1d groupDelay: 67.9842681884766 temperature: 298.16 spectrumSize: 32768 baseFrequency: 300.13 digitalFilter: 67.9842681884766 fieldStrength: 7.049031799154046 numberOfScans: 24 pulseSequence: zg30 spectralWidth: 20.0232508628897 numberOfPoints: 14 relaxationTime: 1 acquisitionTime: 0.001081599999999998 frequencyOffset: 1853.0026200096472 originFrequency: 300.13185300262 pulseStrength90: 22935.77981651376 experimentNumber: 1 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2019-06-19T16:33:02.000Z isFt: true name: wil-190619-180641_oa/1 phc0: 13.77798 phc1: 48.38174 type: NMR Spectrum DECIM: 3328 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TOPSPIN Version 3.2 DSPFVS: 20 nucleus: 1H reverse: false solvent: CDCl3 dimension: 1 increment: 1.5402500663761307 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z828401/0054 experiment: 1d groupDelay: 67.9842681884766 temperature: 298.16 spectrumSize: 32768 baseFrequency: 300.13 fieldStrength: 7.049031799154046 numberOfScans: 24 pulseSequence: zg30 spectralWidth: 20.0232508628897 numberOfPoints: 14 relaxationTime: 1 acquisitionTime: 0.001081599999999998 frequencyOffset: 1853.0026200096472 originFrequency: 300.13185300262 pulseStrength90: 22935.77981651376 experimentNumber: 1 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2019-06-19T16:50:16.000Z isFt: false name: wil-190619-180641_oa/2 phc0: -53.4077 phc1: -3.064588 type: NMR FID DECIM: 1013.33333333333 aqMod: 3 isFid: true tdOff: 0 title: Parameter file, TOPSPIN Version 3.2 DSPFVS: 20 nucleus: 13C reverse: false solvent: CDCl3 dimension: 1 increment: 0.000025333333333333303 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z828401/0054 experiment: 1d groupDelay: 67.9891052246094 temperature: 299.16 spectrumSize: 65536 baseFrequency: 75.467749 digitalFilter: 67.9891052246094 fieldStrength: 7.047530271949235 numberOfScans: 192 pulseSequence: zgpg30 spectralWidth: 261.497817794127 numberOfPoints: 12 relaxationTime: 2 acquisitionTime: 0.0002786666666666663 frequencyOffset: 8376.467332496417 originFrequency: 75.4761254673325 pulseStrength90: 25000 experimentNumber: 2 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2019-06-19T16:50:16.000Z isFt: true name: wil-190619-180641_oa/2 phc0: -53.4077 phc1: -3.064588 type: NMR Spectrum DECIM: 1013.33333333333 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TOPSPIN Version 3.2 DSPFVS: 20 nucleus: 13C reverse: false solvent: CDCl3 dimension: 1 increment: 23.77252889037518 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z828401/0054 experiment: 1d groupDelay: 67.9891052246094 temperature: 299.16 spectrumSize: 65536 baseFrequency: 75.467749 fieldStrength: 7.047530271949235 numberOfScans: 192 pulseSequence: zgpg30 spectralWidth: 261.497817794127 numberOfPoints: 12 relaxationTime: 2 acquisitionTime: 0.0002786666666666663 frequencyOffset: 8376.467332496417 originFrequency: 75.4761254673325 pulseStrength90: 25000 experimentNumber: 2 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2019-06-19T17:00:09.000Z isFt: false name: wil-190619-180641_oa/3 phc0: 142.1428 phc1: -31.9269 type: NMR FID DECIM: 1013.33333333333 aqMod: 3 isFid: true tdOff: 0 title: Parameter file, TOPSPIN Version 3.2 DSPFVS: 20 nucleus: 13C reverse: false solvent: CDCl3 dimension: 1 increment: 0.000025333333333333303 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z828401/0054 experiment: dept groupDelay: 67.9891052246094 temperature: 299.16 spectrumSize: 32768 baseFrequency: 75.467749 digitalFilter: 67.9891052246094 fieldStrength: 7.047530271949235 numberOfScans: 96 pulseSequence: deptsp135 spectralWidth: 261.497817794127 numberOfPoints: 12 relaxationTime: 2 acquisitionTime: 0.0002786666666666663 frequencyOffset: 8376.467332496417 originFrequency: 75.4761254673325 pulseStrength90: 25000 experimentNumber: 3 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2019-06-19T17:00:09.000Z isFt: true name: wil-190619-180641_oa/3 phc0: 142.1428 phc1: -31.9269 type: NMR Spectrum DECIM: 1013.33333333333 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TOPSPIN Version 3.2 DSPFVS: 20 nucleus: 13C reverse: false solvent: CDCl3 dimension: 1 increment: 23.77252889037518 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z828401/0054 experiment: dept groupDelay: 67.9891052246094 temperature: 299.16 spectrumSize: 32768 baseFrequency: 75.467749 fieldStrength: 7.047530271949235 numberOfScans: 96 pulseSequence: deptsp135 spectralWidth: 261.497817794127 numberOfPoints: 12 relaxationTime: 2 acquisitionTime: 0.0002786666666666663 frequencyOffset: 8376.467332496417 originFrequency: 75.4761254673325 pulseStrength90: 25000 experimentNumber: 3 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1
本数据集包含针对样本wil-190619-180641_oa采集的核磁共振(Nuclear Magnetic Resonance, NMR)相关数据,包含自由感应衰减(Free Induction Decay, FID)信号及经傅里叶变换后的NMR谱图,详细采集参数如下:
### 条目1:wil-190619-180641_oa/1
1. 采集时间:2019-06-19T16:33:02.000Z
2. 是否经傅里叶变换:否
3. 数据类型:NMR FID(核磁共振自由感应衰减信号)
4. 零级相位校正参数phc0: 13.77798,一级相位校正参数phc1: 48.38174
5. 抽取因子DECIM: 3328
6. 采集模式aqMod: 3
7. 是否为FID:是
8. 时域偏移tdOff: 0
9. 标题:参数文件,TOPSPIN 版本3.2,DSPFVS: 20
10. 观测核:1H(氢核)
11. 是否反转:否
12. 溶剂:CDCl3(氘代氯仿)
13. 实验维度:1(一维实验)
14. 采样增量:0.00008319999999999985
15. 是否为复数值:是
16. 探头型号:5 mm PABBO BB-1H/D Z-GRD Z828401/0054
17. 实验类型:1d(一维实验)
18. 群延迟:67.9842681884766
19. 实验温度:298.16 K
20. 光谱点数:32768
21. 基频:300.13
22. 数字滤波器参数:67.9842681884766
23. 磁场强度:7.049031799154046
24. 扫描累加次数:24
25. 脉冲序列:zg30
26. 谱宽:20.0232508628897
27. 有效采样点数:14
28. 弛豫延迟时间:1
29. 采集时长:0.001081599999999998
30. 频率偏移量:1853.0026200096472
31. 初始频率:300.13185300262
32. 90°脉冲功率:22935.77981651376
33. 实验编号:1
34. 采集方案:未定义
35. 线性预测区间:0
36. 线性预测系数数量:0
37. 窗函数乘模式:1
该条目下另有经傅里叶变换后的谱图数据:
采集时间:2019-06-19T16:50:16.000Z
是否经傅里叶变换:是
数据类型:NMR Spectrum(核磁共振谱图)
采样增量:1.5402500663761307
其余参数与上述FID数据一致,相位校正参数为phc0: 13.77798,phc1: 48.38174
### 条目2:wil-190619-180641_oa/2
1. 采集时间:2019-06-19T16:50:16.000Z
2. 是否经傅里叶变换:否
3. 数据类型:NMR FID(核磁共振自由感应衰减信号)
4. 零级相位校正参数phc0: -53.4077,一级相位校正参数phc1: -3.064588
5. 抽取因子DECIM: 1013.33333333333
6. 采集模式aqMod: 3
7. 是否为FID:是
8. 时域偏移tdOff: 0
9. 标题:参数文件,TOPSPIN 版本3.2,DSPFVS: 20
10. 观测核:13C(碳十三核)
11. 是否反转:否
12. 溶剂:CDCl3(氘代氯仿)
13. 实验维度:1(一维实验)
14. 采样增量:0.000025333333333333303
15. 是否为复数值:是
16. 探头型号:5 mm PABBO BB-1H/D Z-GRD Z828401/0054
17. 实验类型:1d(一维实验)
18. 群延迟:67.9891052246094
19. 实验温度:299.16 K
20. 光谱点数:65536
21. 基频:75.467749
22. 数字滤波器参数:67.9891052246094
23. 磁场强度:7.047530271949235
24. 扫描累加次数:192
25. 脉冲序列:zgpg30
26. 谱宽:261.497817794127
27. 有效采样点数:12
28. 弛豫延迟时间:2
29. 采集时长:0.0002786666666666663
30. 频率偏移量:8376.467332496417
31. 初始频率:75.4761254673325
32. 90°脉冲功率:25000
33. 实验编号:2
34. 采集方案:未定义
35. 线性预测区间:0
36. 线性预测系数数量:0
37. 窗函数乘模式:1
该条目下另有经傅里叶变换后的谱图数据:
采集时间:2019-06-19T16:50:16.000Z
是否经傅里叶变换:是
数据类型:NMR Spectrum(核磁共振谱图)
采样增量:23.77252889037518
其余参数与上述FID数据一致,相位校正参数为phc0: -53.4077,phc1: -3.064588
### 条目3:wil-190619-180641_oa/3
1. 采集时间:2019-06-19T17:00:09.000Z
2. 是否经傅里叶变换:否
3. 数据类型:NMR FID(核磁共振自由感应衰减信号)
4. 零级相位校正参数phc0: 142.1428,一级相位校正参数phc1: -31.9269
5. 抽取因子DECIM: 1013.33333333333
6. 采集模式aqMod: 3
7. 是否为FID:是
8. 时域偏移tdOff: 0
9. 标题:参数文件,TOPSPIN 版本3.2,DSPFVS: 20
10. 观测核:13C(碳十三核)
11. 是否反转:否
12. 溶剂:CDCl3(氘代氯仿)
13. 实验维度:1(一维实验)
14. 采样增量:0.000025333333333333303
15. 是否为复数值:是
16. 探头型号:5 mm PABBO BB-1H/D Z-GRD Z828401/0054
17. 实验类型:dept(无畸变极化转移增强实验)
18. 群延迟:67.9891052246094
19. 实验温度:299.16 K
20. 光谱点数:32768
21. 基频:75.467749
22. 数字滤波器参数:67.9891052246094
23. 磁场强度:7.047530271949235
24. 扫描累加次数:96
25. 脉冲序列:deptsp135
26. 谱宽:261.497817794127
27. 有效采样点数:12
28. 弛豫延迟时间:2
29. 采集时长:0.0002786666666666663
30. 频率偏移量:8376.467332496417
31. 初始频率:75.4761254673325
32. 90°脉冲功率:25000
33. 实验编号:3
34. 采集方案:未定义
35. 线性预测区间:0
36. 线性预测系数数量:0
37. 窗函数乘模式:1
该条目下另有经傅里叶变换后的谱图数据:
采集时间:2019-06-19T17:00:09.000Z
是否经傅里叶变换:是
数据类型:NMR Spectrum(核磁共振谱图)
采样增量:23.77252889037518
其余参数与上述FID数据一致,相位校正参数为phc0: 142.1428,phc1: -31.9269
提供机构:
nmrXiv
创建时间:
2024-08-14



