Hypervalent Iodine(III) Mediated Synthesis of 3‑Substituted 5‑Amino-1,2,4-thiadiazoles through Intramolecular Oxidative S–N Bond Formation
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https://figshare.com/articles/dataset/Hypervalent_Iodine_III_Mediated_Synthesis_of_3_Substituted_5_Amino-1_2_4-thiadiazoles_through_Intramolecular_Oxidative_S_N_Bond_Formation/3491606
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资源简介:
An efficient synthesis of 3-substituted-5-arylamino-1,2,4-thiadiazoles through intramolecular oxidative S–N bond formation of imidoyl thioureas by phenyliodine(III) bis(trifluoroacetate) is reported. The protocol features a metal-free approach, broad substrate scope, very short reaction times, good to excellent yields, and simple starting materials.
创建时间:
2016-08-01



