Data for: Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty

<p>This dataset includes the measurement data described in the paper "Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty" and additional supplementary data. All data in .csv files except 'Inj1 -- 5' are generated directly by the rheometer software from the rheometer measurements. </p>

<p>Microsoft Excel files:</p>

<ul>
<li>settings.xlsx: Contains settings for all the measurements</li>
</ul>

<p>Comma separated value files:</p>

<ul>
<li>Benchmark-1 -- 4.csv: Oscillatory test at 3 mNm torque amplitude and 1 Hz frequency (Fig.S1)</li>
<li>
<p>Inj1 -- 5.csv: Injection test at 0.025 mL/s (Fig. 7a, 7b)</p>
</li>
<li>
<p>Rh1a.csv: Oscillatory deformation of 0.2\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2a)</p>
</li>
<li>
<p>Rh1b.csv: Oscillatory deformation of 20\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2b)</p>
</li>
<li>
<p>Rh2a.csv: Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz (5 mins) (ii) 20\% strain amplitude, 1 Hz (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz (22 mins) (Fig. 2c)</p>
</li>
<li>
<p>Rh2b.csv: Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz, 23 °C (5 mins) (ii) 20\% strain amplitude, 1 Hz, 23 °C (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz, 37 °C (22 mins) (Fig. 2d)</p>
</li>
<li>
<p>Rh3.csv: Rotational shear stress was applied in steps of (i) 0 Pa (ii) 100 Pa (iii) 0 Pa (iv) 500 Pa (v) 0 Pa (vi) 2000 Pa (vii) 0 Pa, of one minute each, to evaluate creep behaviour. (Fig. 3a)</p>
</li>
<li>
<p>Rh4-1.csv: Rotational shear strain was applied in steps of (i) 0\% (ii) 1\% (iii) 0\%, of two minutes each. (Fig. 3b)</p>
</li>
<li>
<p>Rh4-2.csv: Rotational shear strain was applied in steps of (i) 0\% (ii) 100\% (iii) 0\%, of two minutes each. (Fig. 3b)</p>
</li>
<li>
<p>Rh5-1 -- 3.csv: Amplitude sweep test, where the strain amplitude was gradually increased from 0.01\% to 1000\%. The test was done at 1 Hz frequency (Fig. 3c, 3d)</p>
</li>
<li>
<p>Rh6-1 -- 3.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.01% strain amplitude (Fig. 3e, 3f)</p>
</li>
<li>
<p>Rh6-4 -- 6.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.03% strain amplitude (Fig. 5)</p>
</li>
<li>
<p>Rh6-7 -- 9.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.2% strain amplitude (Fig. 5)</p>
</li>
<li>
<p>Rh6-10.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 200% strain amplitude (Fig. 5)</p>
</li>
<li>
<p>Rh7a-1.csv: Rotational shear rate sweep from 0.001 to 1000 1/s (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh7a-2.csv: Rotational shear rate sweep from 0.01 to 1 1/s (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh7a-3.csv: Rotational shear rate sweep from 0.001 to 0.01 1/s (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh7a-4.csv: Rotational shear rate sweep from 1 to 100 1/s (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh7a-5.csv: Rotational shear rate sweep from 10 to 1000 1/s (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh7b-1.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh7b-2.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh7b-3.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)</p>
</li>
<li>
<p>Rh8-1.csv: Constant rotational shear rate 0.0001 1/s for 20 minutes (Fig. 4c)</p>
</li>
<li>
<p>Rh8-2.csv: Constant rotational shear rate 0.001 1/s for 20 minutes (Fig. 4c)</p>
</li>
<li>
<p>Rh8-3.csv: Constant rotational shear rate 0.01 1/s for 20 minutes (Fig. 4c)</p>
</li>
<li>
<p>Rh8-4.csv: Constant rotational shear rate 0.1 1/s for 20 minutes (Fig. 4c)</p>
</li>
<li>
<p>Rh8-5.csv: Constant rotational shear rate 1 1/s for 20 minutes (Fig. 4c)</p>
</li>
<li>
<p>Rh8-6.csv: Constant rotational shear rate 100 1/s for 20 minutes (Fig. 4c)</p>
</li>
<li>
<p>Rh9.csv: Bone cement was prepared and simply left on the rheometer between the plates while maintaining 1.5 mm gap for 45 minutes without any action.</p>
</li>
<li>
<p>Rh10.csv: Bone cement was prepared and subjected to 15 minutes of rotational 100 1/s shear rate and then 30 minutes of no action on the rheometer.</p>
</li>
</ul>