Details for single-crystal X-ray data collections and structure refinements for the compounds Cd2Pr and Cd3Pr.
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https://figshare.com/articles/dataset/_Details_for_single_crystal_X_ray_data_collections_and_structure_refinements_for_the_compounds_Cd_2_Pr_and_Cd_3_Pr_/993535
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aNONIUS four-circle diffractometer (equipped with a CCD detector and a 300 μm capillary-optics collimator, Mo tube, graphite monochromator; 30 mm crystal-detector distance; rotation angle 2° per image, φ-scans at 14 distinct ω-angles). Structure refinements were performed with program SHELXL (Sheldrick [34]).*513 measured frames, exposure time of 145 seconds per degree.**514 measured frames, exposure time of 165 seconds per degree.
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2015-12-02
