Synthesis and Characterization of N-[2-P(i-Pr)2-4-methylphenyl]2– (PNP) Pincer Tin(IV) and Tin(II) Complexes
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https://figshare.com/articles/dataset/Synthesis_and_Characterization_of_i_N_i_2_P_i_i_i_Pr_sub_2_sub_4_methylphenyl_sub_2_sub_sup_sup_PNP_Pincer_Tin_IV_and_Tin_II_Complexes/2521114
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N-[2-P(i-Pr)2-4-methylphenyl]2– (PNP) pincer complexes of tin(IV) and tin(II), [(PNP)SnCl3] (2) and [(PNP)SnN(SiMe3)2] (3), respectively, were prepared and characterized by X-ray diffraction, solution and solid state NMR spectroscopy, and 119Sn Mössbauer spectroscopy. Furthermore, 119Sn cross polarization magic angle spinning NMR spectroscopic data of [Sn(NMe2)2]2 are reported. Compound 2 is surprisingly stable toward air, but attempts to substitute chloride ligands caused decomposition.
创建时间：
2016-02-20
