SEM & EDX (Zeiss Sigma) of both dropcast and freeze-cast MXene nanoparticles

Microstructure of freeze-cast (FC) and lyophilised Ti3C2Tz aqueous suspensions are imaged with secondary electron microscopy. EDX is deployed on these same samples to verify nanoparticle composition. Dilute Ti3C2Tz aqueous suspensions produced from the same synthesis used in the FC structures are dropcast on silicon wafer in an attempt to produce a particle-size distribution with subsequent image analysis.

See attached .pdf for full data and experiment description.

采用二次电子显微镜对冻结铸造(FC)和冷冻干燥(Ti3C2Tz)水悬浮液的微观结构进行成像。对这些样品应用能量色散X射线光谱(EDX)技术以验证纳米颗粒组成。由与FC结构中使用的相同合成方法制备的稀释Ti3C2Tz水悬浮液被滴铸在硅片上，旨在生成具有后续图像分析的粒子尺寸分布。详见附件.pdf中的完整数据和实验描述。