Synthesis of CF3CH2‑Containing Indolines by Transition-Metal-Free Aryltrifluoromethylation of Unactivated Alkenes
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https://figshare.com/articles/dataset/Synthesis_of_CF_sub_3_sub_CH_sub_2_sub_Containing_Indolines_by_Transition-Metal-Free_Aryltrifluoro_methylation_of_Unactivated_Alkenes/7093370
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With an unactivated double bond as the radical acceptor, allyl amines underwent a metal-free trifluoromethylation/cyclization cascade with CF3SO2Na (Langlois’ reagent), affording CF3CH2-containing indolines and tetrahydroisoquinolines, whose practical syntheses are significant challenges. This protocol features mild conditions, low cost, and a broad substrate scope.
创建时间：
2018-09-17
