Authentication of 4-chloro-3-hydroxy-biphenyl
收藏figshare.com2023-05-30 更新2025-03-23 收录
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https://figshare.com/articles/dataset/Authentication_of_4-chloro-3-hydroxy-biphenyl/10299302/1
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Authentication of 4-chloro-3-hydroxy-biphenyl by 1H NMR, 13C NMR, and GC-MS. The title compound was synthesized by demethylation of 3-methoxy-4-chloro-biphenyl in the presence of BBr3. The purity (>99%) of the compound was determined based on relative peak area by GC-MS.
通过1H NMR、13C NMR和GC-MS对4-氯-3-羟基联苯进行鉴定。标题化合物在BBr3存在下，通过3-甲氧基-4-氯联苯的脱甲基反应合成。该化合物的纯度（>99%）基于GC-MS相对峰面积测定。
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