Host–Guest Behavior of a Heavy-Atom Heterocycle Re4(CO)16(μ-SbPh2)2(μ-H)2 Obtained from a Palladium-Assisted Ring Opening Dimerization of Re2(CO)8(μ-SbPh2)(μ-H)
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https://figshare.com/articles/dataset/Host_Guest_Behavior_of_a_Heavy_Atom_Heterocycle_Re_sub_4_sub_CO_sub_16_sub_SbPh_sub_2_sub_sub_2_sub_H_sub_2_sub_Obtained_from_a_Palladium_Assisted_Ring_Opening_Dimerization_of_Re_sub_2_sub_CO_sub_8_sub_SbPh_sub_2_sub_H_/2179936
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The heavy-atom heterocycle Pd[Re2(CO)8(μ-SbPh2)(μ-H)]2 (5) has been synthesized by the palladium-catalyzed ring-opening cyclodimerization of the three-membered heterocycle Re2(CO)8(μ-SbPh2)(μ-H) (3). The Pd atom occupies the center of the ring. The Pd atom in 5 can be removed reversibly to yield the palladium-free heterocycle [Re2(CO)8((μ-SbPh2)(μ-H)]2 (6).
创建时间：
2016-02-13
