Epidote - Sample 1 NanED Round Robin, Data ESR3

General information:

Project

NanED (www.naned.eu)

ESR Project

ESR3

Instrumental:

Instrument

FEI TECNAI

Radiation source

FEG

Accelerating voltage

200 kV

Wavelength

0.0251 Å

Acquisiton Method

SAED

Detector

Eagle – CCD Camera

Number of pixels in the image

2048 x 2048

Calibration constant (not corrected for Effective Camera length)

0.00182 Å-1/pixel

Sample description:

Name

Epidote

Chemical composition

Ca2FexAl3-xSi3O13H

Experimental:

Data Type

Electron diffraction data - 3D ED

Data collection method

Stepwise

Temperature (K) used during data collection

293 K

Number of crystals contributing to the data set

1

Number of experimental frames

351

tilt range, tilt step

-35° to +35°, 0.2°

Exposure time per frame

1s

Software:

Software used for the data collection

TIA

Software used for processing

PETS2

Software used for Solution

Jana

Software used for refinement

Olex2