Four sweep cubic insulin data set recorded using dose mode (1MGy / scan) on Diamond Light Source beamline i04
收藏Zenodo2023-09-25 更新2026-04-07 收录
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https://zenodo.org/record/8376817
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Four sweep cubic insulin data set recorded on Diamond Light Source beamline i04 as part of routine testing. Data were collected with four full 360° scans / 0.1° / image to give a total of 1MGy / scan i.e. "carefully" to avoid problems of obvious radiation damage. The beam size was adjusted to be about the same as the crystal, spreading the dose uniformly across the sample. Processing using my "standard DIALS script" gives nice data to 1.2Å: <pre><code> Overall Low High High resolution limit 1.20 3.26 1.20 Low resolution limit 55.07 55.13 1.22 Completeness 100.0 100.0 100.0 Multiplicity 150.2 155.4 76.0 I/sigma 40.8 295.5 0.4 Rmerge(I) 0.075 0.027 7.170 Rmerge(I+/-) 0.075 0.026 7.127 Rmeas(I) 0.076 0.027 7.218 Rmeas(I+/-) 0.075 0.027 7.220 Rpim(I) 0.006 0.002 0.815 Rpim(I+/-) 0.008 0.003 1.140 CC half 1.000 1.000 0.335 Anomalous completeness 100.0 100.0 100.0 Anomalous multiplicity 77.7 84.8 38.9 Anomalous correlation 0.499 0.680 -0.005 Anomalous slope 0.626 dF/F 0.031 dI/s(dI) 0.761 Total observations 3709553 203869 91461 Total unique 24699 1312 1204</code></pre> Data shared to allow use in tutorials etc. as well as a reference for future data handling questions.
提供机构:
Bertram, Felicity; Winter, Graeme; Aragao, David
创建时间:
2023-09-25



