Synthesis of α,α-Disulfenylated Aldehydes via Oxidative Transformation of Tertiary Amines
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https://figshare.com/articles/dataset/Synthesis_of_Disulfenylated_Aldehydes_via_Oxidative_Transformation_of_Tertiary_Amines/2112577
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A method for the copper-catalyzed regioselective β-functionalization of tertiary amines with thiophenols has been developed. The control experiments and primary studies show that a thiyl radical is involved in the reaction, and the method provides a novel and direct approach to synthesize C(sp3)–S bonds without a directing group under ligand-free conditions.
创建时间：
2016-02-12
