A Novel Recyclable Sulfur Monoxide Transfer Reagent
收藏NIAID Data Ecosystem2026-03-06 收录
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https://figshare.com/articles/dataset/A_Novel_Recyclable_Sulfur_Monoxide_Transfer_Reagent/3740439
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资源简介:
Trisulfide 2-oxide 11 has been prepared from disulfide 9 via reduction to the corresponding dithiol and subsequent trapping with thionyl
chloride. Heating trisulfide oxide 11 in the presence of dienes results in transfer of sulfur monoxide to form cyclic unsaturated sulfoxides 13
in good to excellent yields, along with recovery of disulfide 9. A Pummerer reaction can be used to convert the cyclic sulfoxides into thiophenes.
创建时间:
2016-08-20



