Kinetic evaluation of a flow mode process of 4-aminophenol synthesis

The colletion contains a set of data related to the design and optimization of 4-aminophenol synthesis through the optimization of flow-mode coninous process of 4-nitrophenol hydrogenation. The process development involved 3D-printing of tubular reactors as well as systematic evaluation of catalysts morphology on their catalytic activity and performance. In this context, a particular focus has been put on the reactors capacity, reaction kinetics, and the mechanism of catalyst deactivation.The research was carried out within OPUS 25 project (UMO-2023/49/B/ST8/01029) granted by National Science Center (Poland). Aim of the project is to develop new generation of catalytical technology for the production of aromatic amines.The set of data contains:Pore size distribution (PSD) of matrices applied as catalysts base. 3DUV-Vis spectra recorded during catalytic reduction of 4-nitrophenol (batch mode).Reactors' breakthrough curves of the catalytic reduction of 4-nitrophenol (flow mode).XPS Re 4f spectra of the catalysts samples before and after catalytic process.Reactor's breakthrough curves in the function of varied reagents residence time (kinetics optimization).Total Ion Chromatogram and mass spectra of reactor's effluent collected as the stage of process validation.