EPR spectra of Nitrobenzene with Lewis bases

Electron paramagnetic data for the characterisation of the radical formed upon reaction of nitrobenzene and multiple Lewis bases.

The folder structure is as follows:

Base
├── Concentration│   ├── Nitrobenzene_Base_molar_ratio
│   │    ├── data.DSC│   │    ├── data.DTA│   │    ├── fit.DSC
│   │    └── fit.DTA│   ├── Nitrobenzene_Base_Chelate_molar_ratio
│   │    ├── data.DSC│   │    ├── data.DTA│   │    ├── fit.DSC
│   │    └── fit.DTA

Where Base is the employed Lewis base to run the experiment (tBuLi, LDA, NaiPrCp, LiOtBu, NaOtBu, KOtBu, LiHMDS, NaHMDS, KHMKDS)├──Concentration is the milliMolar concentration of nitrobenzene, │   ├── Nitrobenzene_Base_molar_ratio indicates the employed molar ratio between nitrobenzene and base, and │   ├── Nitrobenzene_Base_Chelate_molar_ratio, if present, indicates the employed molar ratio between nitrobenzene, base and a ligand (222 Cryptand, 15-Crown-5, 12-Crown-4) used to chelate the alkali metal.Inside each folder, the raw *.DSC and *.DTA Bruker files are given, and if available, their fit as well.The filenames contain the power attenuation (dB), modulation amplitude (Gauss) and number of scans used to record the data.