Data collection and refinement statistics for structures reported in this work.
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*Values in parenthesis are for the highest-resolution shell.†Rmerge(I) = (Σhkl Σj |Ihkl,j−〈Ihkl〉|)/(Σhkl Σj Ihkl,j) where 〈Ihkl〉 is the average intensity of j symmetry-related observations of reflections with Miller indices hkl.#CC1/2 = percentage of correlation between intensities from random half-datasets.‡Rwork = Σhkl|F(obs)−F(calc)|/Σhkl|F(obs)|; 5% of the data that were excluded from the refinement were used to calculate Rfree.
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2015-12-02
