The morphology of vanadate glass-ceramics containing BaTiO3 measured with the use of AFM
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The structure of vanadate glass-ceramics doped with BaTiO3 was measured by AFM technique. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated (573 K) brass plate and pressed by another plate. A subset of as-quenched samples was heat treated in air at the temperature of 633 K (close to the crystallization temperature) for 6 h and cooled with the furnace. The structure has been studied by atomic force microscopy with NT-MDT Ntegra AFM microscope on fresh fractured samples.
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Natalia Anna Wójcik
