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青蟹(膏)铜质量安全检测数据

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浙江省数据知识产权登记平台2023-10-14 更新2024-05-08 收录
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本数据主要用于监测三门青蟹(膏)铜指标的变化情况,用于监管部门加强对三门青蟹养殖经营过程的监管。1.样品来源:本项目抽检的青蟹全部来源于三门县流通环节市场主体经营的青蟹,检测部位是膏。 2.数据检测:青蟹样品经处理并取出蟹膏,经消解后,由电感耦合等离子体质谱仪测定,以铜元素特定质量数定性,采用外标法,以铜元素质谱信号与内标元素质谱信号的强度比与铜元素的浓度成正比进行定量分析。 3.数据判定:铜含量的计算,x=(ρ-ρ0)×v×f/m。试样铜含量,单位为毫克每千克或毫克每升(mg/kg或 mg/L);ρ试样溶液中被测元素质量浓度,单位为毫克每升(mg/L);ρ0试样空白液中被测元素质量浓度,单位为毫克每升(mg/L);V试样消化液定容体积,单位为毫升(ml);f试样稀释倍数;m试样称取质量或移取体积,单位为克或毫升(g或 ml)。计算结果保留三位有效数字。含铜量<3mg/1000g的可食;3-5mg/1000g的少食。4.数据应用:通过抽检数据分析研判,对通过抽检结果加强该区域水质、土壤的检测以及养殖过程的监管,提升三门青蟹质量水平。

This dataset is primarily used to monitor changes in the copper content index of the cream (roe) of Sanmen green crabs, to help regulatory authorities strengthen supervision over the breeding and operation processes of Sanmen green crabs. 1. Sample Source: All sampled green crabs in this project were sourced from market entities operating in the circulation links of Sanmen County, with the tested tissue being the crab cream. 2. Data Testing: After processing the green crab samples and extracting their crab cream, the samples were digested and then determined by inductively coupled plasma mass spectrometry (ICP-MS). Qualitative analysis was conducted based on the specific mass number of copper element, while quantitative analysis was performed using the external standard method, where the intensity ratio of the mass spectrum signal of copper element to that of the internal standard element is proportional to the concentration of copper element. 3. Data Judgment: The calculation formula for copper content is x = (ρ - ρ₀) × v × f / m. The copper content of the test sample is expressed in milligrams per kilogram or milligrams per liter (mg/kg or mg/L), where: ρ: mass concentration of the detected element in the sample solution, unit: mg/L; ρ₀: mass concentration of the detected element in the sample blank solution, unit: mg/L; V: constant volume of the sample digested solution, unit: milliliters (ml); f: dilution factor of the sample; m: weighed mass or pipetted volume of the test sample, unit: g or ml. The calculation results shall be rounded to three significant figures. Samples with copper content less than 3 mg/1000g are edible; those with copper content ranging from 3 to 5 mg/1000g should be consumed sparingly. 4. Data Application: Through the analysis and assessment of the sampling inspection data, the detection of water quality and soil in this region and the supervision of the breeding process can be strengthened based on the sampling results, so as to elevate the quality level of Sanmen green crabs.
提供机构:
三门县食品药品检验检测中心(三门县药品不良反应监测中心)
创建时间:
2023-09-22
搜集汇总
数据集介绍
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特点
该数据集记录了青蟹(膏)中铜含量的检测数据,共102条,数据来源于企业,采用电感耦合等离子体质谱仪测定,主要用于监测三门青蟹(膏)铜指标的变化,帮助监管部门加强养殖经营过程的监管。
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