EGB-Promoted Electrochemical Synthesis of 6-Thioxo-[1,3,5]- Triazinane-2,4 Dione Derivatives
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https://tandf.figshare.com/articles/dataset/EGB_Promoted_Electrochemical_Synthesis_of_6_Thioxo_1_3_5_Triazinane_2_4_Dione_Derivatives/3121894/1
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资源简介：
A simple method for the synthesis of 6-Thioxo-[1,3,5]-triazinane-2,4-dione derivatives was reported. The electrogenerated cyanomethyl base obtained from electroreduction of neat acetonitrile assisted the reaction between thiourea derivatives and alkyl or aryl isocyanate. This protocol had the advantage of giving good yields using mild conditions. The obtained products have been identified according to their spectroscopic data, by mass spectrometry and high-resolution mass spectra or elemental analysis.
提供机构：
Taylor & Francis
创建时间：
2016-03-22
