Photo-Biocatalytic Sequential One-Pot/Two-Step Synthesis of Optically Active (R)- and (S)-1-Phenylethanols from α-Methylstyrenes

The deposited dataset includes: (i) free induction decay (FID) files, acquisition parameters, and processing details for the recorded 1H, 13C{1H}, and 19F NMR spectra of a set of compounds (e.g., secondary alcohols), and (ii) raw, unprocessed HPLC analytical data of racemic alcohols, and their respective optically enriched enantiomeric forms. This data consists of supplementary data for an article entitled: "Photo-Biocatalytic Sequential One-Pot/Two-Step Synthesis of Optically Active (R)- and (S)-1-Phenylethanols from α-Methylstyrenes", which has been submitted to the European Journal of Organic Chemistry (EJOC) journal (Online ISSN: 1099-0690) on 29 May 2026. This research was funded by the National Science Centre, Poland within the framework of the project "OPUS 24" (Grant No. 2022/47/B/ST4/00139).