Synthesis of Imidazo[1,2‑a]pyridines: “Water-Mediated” Hydroamination and Silver-Catalyzed Aminooxygenation
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https://figshare.com/articles/dataset/Synthesis_of_Imidazo_1_2_i_a_i_pyridines_Water_Mediated_Hydroamination_and_Silver_Catalyzed_Aminooxygenation/2447605
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Aqueous syntheses of methylimidazo[1,2-a]pyridines without any deliberate addition of catalyst are reported. Imidazo[1,2-a]pyrazine and imidazo[2,1-a]isoquinoline were also obtained in good yields under similar conditions. With acetonitrile as solvent, Ag-catalyzed intramolecular aminooxygenation produced imidazo[1,2-a]pyridine-3-carbaldehydes in moderate to good yields.
创建时间：
2016-02-20
