Kinetic and process data for continuous flow hydrogenation of nitroaromatic compounds in a 3D-printed packed red reactor

The colletion contains a set of data related to the design and optimization of packed bed reactor (PBR) for the continous reduction of nitroaromatic compounds, including 4-nitrophenol, nitrobenzene, 2-nitroaniline, 4-nitroaniline, and 2,4,6-trinitropjenol. The development of PBR involved 3D-printing using stereolitography as well as the in-depth assessment of process parameters focused on reactors capacity and reaction kinetics.The research was carried out within Sonata 16 project (UMO-2020/39/D/ST8/01352) granted by National Science Center (Poland). Aim of the project is to develop new generation of catalytical-separation technology for the simultaneous hydrogenation of nitroaromatic compounds and extraction of resulting from the process aromatic amines.The set of data contains:3D STL models with the column designUV-Vis spectra recorded during catalytic reduction of 4-nitrophenol, nitrobenzene, 2-nitroaniline, 4-nitroaniline, and 2,4,6-trinitrophenol.XPS spectra of the samples containing rhenium nanoparticles.Raw HRTEM/HAAFD images obtained during transmission electron microscopy analysis.Low temperature nitrogen adsorption/desorption isotherms.