Metal-Free Annulation of 2‑Nitrobenzyl Alcohols and Tetrahydroisoquinolines toward the Divergent Synthesis of Quinazolinones and Quinazolinethiones
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https://figshare.com/articles/dataset/Metal-Free_Annulation_of_2_Nitrobenzyl_Alcohols_and_Tetrahydroisoquinolines_toward_the_Divergent_Synthesis_of_Quinazolinones_and_Quinazolinethiones/17263694
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资源简介：
A simple metal-free method for the
synthesis of quinazolinones
from commercially available 2-nitrobenzyl alcohols and tetrahydroisoquinolines
is developed. The reaction conditions were tolerant of an array of
functionalities such as halogen, tertiary amine, protected alcohol,
and ester groups. Under nearly identical conditions, quinazolinethiones
were obtained in the presence of elemental sulfur and suitable mediators.
创建时间：
2021-12-17
