Data underlying the publication: Activation of Prussian blue analogues: Temperature effects on structure, porosity, and open metal site accessibility

This dataset support the study of activation of three ferricyanide-based Prussian blue analogues (PBAs) using a N2-based activation procedure. The research aims to elucidate whether activation using N2 rather than vacuum is possible for these PBAs and what structural effects the activation temperature has on material properties. The dataset includes adsorption (N2, CO2, H2O, and CO), DRIFTS, PXRD, SEM, TEM, and TGA.

本数据集支撑针对三种铁氰化物基普鲁士蓝类似物（Prussian blue analogues, PBAs）的氮气活化工艺相关研究。本研究旨在阐明两个核心问题：其一，相较于真空活化，采用氮气对该类普鲁士蓝类似物进行活化是否可行；其二，活化温度对材料性能存在何种结构层面的影响。本数据集涵盖氮气（N₂）、二氧化碳（CO₂）、水（H₂O）与一氧化碳（CO）的吸附表征数据，同时包含漫反射红外傅里叶变换光谱（DRIFTS）、粉末X射线衍射（PXRD）、扫描电子显微镜（SEM）、透射电子显微镜（TEM）以及热重分析（TGA）的相关测试数据。