Bubbles enable volumetric negative compressibility in metastable elastocapillary systems

This data set contains experimental data related to the article Bubbles enable volumetric negative compressibility in metastable elastocapillary systems, https://doi.org/10.1038/s41467-024-49136-w.In particular, crystallographic data for ZIF-67 MOF during water intrusion-extrusion:1. ZIF67.ODS - dependance of latice parameter of ZIF-67 and compressibility on pressure for both intrusion and extrusion processes2. Original data files from APS facility obtained during water intrusion-extrusion into-from ZIF-67:1) ZIF-67_3_RT_d600-00000-00001.dat - as loaded sample2) ZIF-67_3_90C_act_d600-00003.dat - the sample after activation at 90C and measured at 90C3) ZIF-67_3_5C_H2O_d600-00000.dat - the sample at 5C in H2O no pressure applied4) ZIF-67_3_d600_10bar_5C_H2O_int-00003.dat - the sample at 5C in H2O under 10 bar of pressure5) ZIF-67_3_d600_170bar_5C_H2O_int-00003.dat - the sample at 5C in H2O under 170 bar of pressure6) ZIF-67_3_d600_300bar_5C_H2O_int-00003.dat - the sample at 5C in H2O under 300 bar of pressure