EBEC-MicroED: Static electron diffraction movies collected at different incident flux on a direct electron detector (DE Apollo) on crystals of (S,S) Jacobsen's salen ligand and Co(II) porphyrin, and diffraction tilt series recorded on the DE Apollo and CetaD detector for the same crystals of Jacobsen's Ligand
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https://zenodo.org/record/13716389
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资源简介:
This record contains static diffraction movies recorded from crystals of (S,S) Jacobsen's salen ligand, and crystals of Co(II) meso-tetraphenyl porphyrin, using a direct electron detector (DE Apollo) in counting mode. Data were acquired at varying different incident flux settings, referred to as "spotsize11" or "spot11" (0.01 electrons per square Angstoms per second), "spotsize10" or "spot10" (0.03 electrons per square Angstrom per second), "spotsize9" or "spot9" (0.045 electrons per square angstrom per second)", and "spotsize8" or "spot8" (0.084 electrons per sqaure Angstrom per second. For each compound these trials, the same crystal ("crystal1", "crystal2", etc.) was conserved across a dose series, and illuminated at each incident flux from lowest to highest in sequence.
Additionally, this record contains diffraction tilt series acquired from crystals of (S,S) Jacobsen's ligand, first on the Ceta D and next on the DE Apollo, rotating at 2 degrees per second with an incident flux of either 0.01 or 0.045 electrons per square Angstrom per second.
All data is saved in mrc file format, with the exception of movies from the Ceta D, which are saved in ser file format.
创建时间:
2024-09-06



