Synthesis of a Novel Two-Dimensional Antimony Sulfide, [C<sub>4</sub>H<sub>10</sub>N]<sub>2</sub>[Sb<sub>8</sub>S<sub>13</sub>]·0.15H<sub>2</sub>O, and Its Structure Solution Using Synchrotron/Imaging Plate Data
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A novel antimony sulfide, [C4H10N]2[Sb8S13]·0.15H2O, was synthesized hydrothermally, and its structure was determined from data collected using a synchrotron/imaging plate system. The new compound consists of centrosymmetric Sb16S264- planar clusters. Each cluster is connected to four others through two edge-sharing and two corner-sharing SbS3 pyramids, forming an extended sheet. The protonated pyrrolidine molecules reside between the parallel stacked sheets. The structure is triclinic (space group P1̄) with a = 6.929(2) Å, b = 16.747(2) Å, c = 17.976(4) Å, α = 94.84(1°), β = 95.41(1)°, and γ = 125.28(1)°.
创建时间：
2016-08-17
