α-ZrP层状纳米片的修饰改性及其摩擦学性能

采用一步水热法制备了阳离子表面活性剂修饰改性的α-磷酸锆(α-ZrP)纳米片. 利用X-射线衍射仪、傅里叶变换红外光谱仪、拉曼光谱仪、场发射扫描电镜和透射电子显微镜对α-ZrP纳米片在表面活性剂修饰前后的组成、晶体结构以及微观形貌进行了表征分析和观察，并对改性前后的α-ZrP在合成基础油PAO-6中的分散稳定性进行了对比分析，利用SRV-Ⅳ型微动摩擦磨损试验机对含有改性α-ZrP纳米片的PAO-6润滑油的摩擦学性能进行了研究. 结果表明：表面改性的α-ZrP纳米片在PAO-6润滑油中具有良好的分散稳定性，其作为添加剂时可显著提高润滑油的极压性能和抗磨损性能.Cationic surfactant-modified α-zirconium phosphate (α-ZrP) nanosheets were prepared via a one-step hydrothermal method. The composition, crystal structure and microscopic morphology of α-ZrP nanosheets before and after surfactant modification were characterized and observed using X-ray diffractometer (XRD), Fourier transform infrared spectrometer (FT-IR), Raman spectrometer, field emission scanning electron microscope (FESEM) and transmission electron microscope (TEM). Additionally, the dispersion stability of α-ZrP before and after modification in synthetic base oil PAO-6 was comparatively analyzed. The tribological properties of PAO-6 lubricating oil containing modified α-ZrP nanosheets were investigated using an SRV-IV fretting friction and wear tester. The results show that the surface-modified α-ZrP nanosheets exhibit excellent dispersion stability in PAO-6 lubricating oil, and can significantly improve the extreme pressure performance and anti-wear performance of the lubricating oil when used as an additive.

搜集汇总

背景与挑战

背景概述

该数据集研究了α-磷酸锆层状纳米片通过阳离子表面活性剂修饰改性后的性能，重点关注其在PAO-6润滑油中的分散稳定性和摩擦学特性。实验采用一步水热法制备纳米片，并通过多种表征手段分析修饰效果，结果表明改性后的纳米片作为润滑油添加剂能显著提升极压性能和抗磨损性能。数据集来自中国科学院兰州化学物理研究所，涉及摩擦学领域，提供开放获取以支持相关科研应用。