LC-MicroED: TEM-EELS spectra and corresponding images recorded from room-temperature liquid cell MicroED samples
收藏资源简介:
This deposition contains EELS spectra in DM4 (Gatan Inc.) format acquired at a TFS Spectra at 300 keV on a Gatan Continuum CMOS detectorDirect Electron detector, at room temperature (298 K), from carbon "sandwich" liquid cell samples. The subdirectory "EELS_water-LC" contains EELS spectra and corresponding images of the same illuminated region from water and dry regions of the same sample (denoted in each file name). The subdirectories "EELS_ZnHistidine_LC-wet" and "EELS_ZnHistidine_LC-dry" contain EELS spectra and corresponding TEM images from sample regions adjacent to Zn-L-histidine microcrystals in carbon liquid cells, one freshly prepared with a microcrystal suspension and containing solvated crystals (wet) and one allowed to fully dessicate and containing only dried out material (dry). Additionally, this deposition contains low-magnification TEM images of the same LC sample of a suspension of AVAAGA microcrystals in aqueous suspension, first recorded with the sample hydrated and next recorded once the sample was allowed to fully dessicate in a vacuum chamber.



