A Photocycloaddition/Fragmentation Approach toward the 3,12-Dioxatricyclo[8.2.1.06,13]tridecane Skeleton of Terpenoid Natural Products
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https://figshare.com/articles/dataset/A_Photocycloaddition_Fragmentation_Approach_toward_the_3_12_Dioxatricyclo_8_2_1_0_sup_6_13_sup_tridecane_Skeleton_of_Terpenoid_Natural_Products/2673964
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Starting from tetronate 1 (R = CH2OH), a short photochemical access to the 3,12-dioxatricyclo[8.2.1.06,13]tridecane-skeleton 2 of briarellin and asbestinin diterpenes has been explored. In the course of these studies, a number of surprising observations were made. For example, a two-step reaction pathway to the bicyclic ketolactone 3 was discovered, which is based on tetronate 1 (R = COOMe).
创建时间：
2016-02-23
