Single-crystal 3D electron diffraction dataset for urea
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https://repod.icm.edu.pl/citation?persistentId=doi:10.18150/A3WJKN
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资源简介：
Electron diffraction dataset collected from urea (Sigma-Aldrich) micro crystals obtained by slow evaporation using the water solution.Microscope: Thermo Fisher Scientific 200kV Glacios Transmission Electron Microscope (Cryomicroscopy and Electron Diffraction Core Facility at the Centre of New Technologies, University of Warsaw, Poland)Camera: Ceta-D camera (bin 2x2, rolling shutter, noise reduction mode)Collection Software: EPU-D (Thermo Fisher), SMV formatCollection Parameters: 200keV, -193C, 50um C2, gun lens 8, spot size 11, extraction voltage 3850V, parallel beam, beam diameter ~1.7 um, beam stop inserted, calibrated camera length 644 mm (670 in UI), oscillation per frame 1.0 deg, 0.5 s exposure time, tilt speed 2.0 deg/s, rotation -50 to +50 deg, total dose ~3.6 e/A2Grid: lacey carbon Cu 200 mesh glow discharged for 60s at 25mASample: ureaStructure: IAM refinement: CCDC 2308752, TAAM refinement: CCDC 2308753
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RepOD
创建时间：
2023-11-09
