One-Pot Synthesis of [(C6F5)2BH2]− from C6F5MgBr/BH3·SMe2 and Its in Situ Transformation to Piers’ Borane
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https://figshare.com/articles/dataset/One_Pot_Synthesis_of_C_sub_6_sub_F_sub_5_sub_sub_2_sub_BH_sub_2_sub_sup_sup_from_C_sub_6_sub_F_sub_5_sub_MgBr_BH_sub_3_sub_SMe_sub_2_sub_and_Its_in_Situ_Transformation_to_Piers_Borane/2649628
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Depending on the crystallization procedure, the one-pot reaction between 2 C6F5MgBr, 1 BH3·SMe2, and 1 Me3SiCl furnishes the hydridoborate salts [Mg2(Et2O)3Br2Cl][(C6F5)2BH2] and [Mg(Et2O)2][(C6F5)2BH2]2, both of which are convenient starting materials for the in situ generation of Piers’ borane (C6F5)2BH.
创建时间：
2016-02-23
