Preparation of 6,13-Bis(trimethylsilyl)pentacene and Formation of Second-Ring Diels−Alder Adduct of Pentacene
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https://figshare.com/articles/dataset/Preparation_of_6_13_Bis_trimethylsilyl_pentacene_and_Formation_of_Second_Ring_Diels_Alder_Adduct_of_Pentacene/2699896
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6,13-Bis(trimethylsilyl)pentacene was synthesized by a coupling reaction of bicyclic dilithiobutadiene with diiodonaphthalene followed by aromatization. Diels−Alder reaction of 6,13-bis(trimethylsilyl)pentacene with dienophiles afforded the corresponding second-ring adducts. Elimination of two silyl groups gave the second-ring Diels−Alder adducts of parent pentacene.
创建时间：
2016-02-24
