Preparation and Crystallographic Characterization of C60{η1‑Ru(CO)2(η5‑C5H5)}2: A Locally Crowded Organometallic Fullerene Without the Usual η2‑Bonding
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https://figshare.com/articles/dataset/Preparation_and_Crystallographic_Characterization_of_C_sub_60_sub_sup_1_sup_Ru_CO_sub_2_sub_sup_5_sup_C_sub_5_sub_H_sub_5_sub_sub_2_sub_A_Locally_Crowded_Organometallic_Fullerene_Without_the_Usual_sup_2_sup_Bonding/2318167
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The reaction of {(η5-C5H5)Ru(CO)2}2 with C60 in toluene solution under thermal or photolytic conditions produces C60{η1-Ru(CO)2(η5-C5H5)}2, whose structure has been determined by single crystal X-ray diffraction. The two Ru(CO)2(η5-C5H5) units are bound at the opposite ends of a hexagon on the fullerene surface and are closely intertwined.
创建时间：
2016-02-18
