TMCL_DMPC_Ca
收藏DataCite Commons2026-01-16 更新2026-05-04 收录
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This dataset contains NMR spectra obtained for the sample -TMCL_DMPC_Ca Nucleus: 1H NMR Solvent: H2O+D2O NMR Probe: H8609_0043 (PH MAS 500WB BL4 X/Y/H DVT) NMR Pulse Sequence: null Temperature: 309.5112 Observed Frequency: 500.248 Magnetic Field Strength: 11.749122218330188 Number of Scans: 2 NMR Pulse Sequence: onepulse Spectral Width: 19.9900085939046 Number of Data Points: 3006 Relaxation Delay: 5 Observed Frequency: 500.24991 Nucleus: 31P NMR Solvent: H2O+D2O NMR Probe: H8609_0043 (PH MAS 500WB BL4 X/Y/H DVT) NMR Pulse Sequence: 1d Temperature: 307.9882 Observed Frequency: 202.504102 Magnetic Field Strength: 11.745385617451017 Number of Scans: 256 NMR Pulse Sequence: NEA_zg30bbdec Spectral Width: 201.284167395372 Number of Data Points: 5702 Relaxation Delay: 8 Observed Frequency: 202.504102 Nucleus: 31P NMR Solvent: H2O+D2O NMR Probe: H8609_0043 (PH MAS 500WB BL4 X/Y/H DVT) NMR Pulse Sequence: 1d Temperature: 307.9982 Observed Frequency: 202.504102 Magnetic Field Strength: 11.745385617451017 Number of Scans: 1024 NMR Pulse Sequence: NEA_zg30bbdec Spectral Width: 201.284167395372 Number of Data Points: 4072 Relaxation Delay: 6 Observed Frequency: 202.504102
TMCL(14.0mg,1.0 eq.) andDMPC(14.9mg,2.0eq.) weredissolvedwith1mlchloroform:methanol
(7:3, v/v) in an eppendorf vial. A solution of NaOH (0.9mg, 2.0eq.), CaCl2 (0.3mg, 0.25eq.) and
BOH3 (0.7mg, 1.0eq.) in 150µl methanol was prepared and added to the Eppendorf vial. The
solvent was evaporated at 40°C under a constant stream of argon and the predried sample was
freeze-dried over night. 35.6µl degassed water was added and the Eppendorf was stored at 50°C
for one day. Lost water was added and the sample was mixed thoroughly with a steel rod. After
another three days of equilibration the sample was again mixed before packing the insert.
提供机构：
nmrXiv
创建时间：
2026-01-16
