Dataset for synthesis and authentication of 3,3'-dichlorobiphenyl-4-ol (4-OH-PCB 11)
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下载链接：
https://iro.uiowa.edu/esploro/outputs/dataset/9984269958602771
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资源简介：
3,3'-Dichlorobiphenyl-4-ol (4-OH-PCB 11) was synthesized from 4-bromo-2-chloroanisole and 3-chlorobenzene boronic acid using the Suzuki-coupling reaction with Pd2(dba)3 and 2-dicyclohexylphosphino-2',6'-dimethoxybiphenyl (DPDB) as the catalyst, followed by demethylation of 3,3'-dichloro-4-methoxybiphenyl (4-MeO-PCB11) with borontribromide (BBr3). The intermediate compounds and final product were characterized and authenticated.
提供机构：
University of Iowa
创建时间：
2022-07-06
