Synthesis of 2,8-Dioxabicyclo[3.3.1]nonane Derivatives via a Sequential Knoevenagel Condensation and Hetero-Diels–Alder Reaction in an Aqueous Medium
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https://figshare.com/articles/dataset/Synthesis_of_2_8_Dioxabicyclo_3_3_1_nonane_Derivatives_via_a_Sequential_Knoevenagel_Condensation_and_Hetero_Diels_Alder_Reaction_in_an_Aqueous_Medium/2352712
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Utilizing aldehyde-substituted vinylogous carbonates and 1,3-diketones, a simple protocol is presented for the synthesis of 2,8-dioxabicyclo[3.3.1]nonane derivatives via Knoevenagel condensation followed by a hetero-Diels–Alder reaction under green reaction conditions. The structure of a key product is unequivocally confirmed by X-ray crystallography.
创建时间：
2016-02-18
