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Identification of the Side Products That Diminish the Yields of the Monoamidated Product in Metal-Catalyzed C–H Amidation of 2‑Phenylpyridine with Arylisocyanates

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Figshare2020-01-23 更新2026-04-28 收录
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https://figshare.com/articles/dataset/Identification_of_the_Side_Products_That_Diminish_the_Yields_of_the_Monoamidated_Product_in_Metal-Catalyzed_C_H_Amidation_of_2_Phenylpyridine_with_Arylisocyanates/11698374
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The Ru­(II)-catalyzed amidation of 2-arylpyridines with aryl isocyanates via C–H bond activation is less efficient than described previously, due to the formation of a series of side products, which were readily identified using direct infusion electrospray mass spectrometry and high-performance liquid chromatography–mass spectrometry.
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2020-01-23
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