Asymmetric Diels–Alder Reaction Involving Dynamic Enantioselective Crystallization
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https://figshare.com/articles/dataset/Asymmetric_Diels_Alder_Reaction_Involving_Dynamic_Enantioselective_Crystallization/6483977
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资源简介：
Asymmetric
Diels–Alder reaction was achieved under achiral
conditions. Reaction of prochiral 2-methylfuran and N-phenylmaleimide in heptane or hexane solution at 80 °C efficiently
gave a conglomerate crystal of exo-type Diels–Alder
adduct selectively, and continuous suspension of the reaction mixture
with glass beads promoted attrition-enhanced deracemization, leading
to an optically active exo-adduct in 90% ee.
创建时间：
2018-06-11
