Hydroxyalkylation of Conjugated Nitroalkenes with Activated Nonenolizable Carbonyl Compounds
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https://figshare.com/articles/dataset/Hydroxyalkylation_of_Conjugated_Nitroalkenes_with_Activated_Nonenolizable_Carbonyl_Compounds/3233062
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资源简介：
The Morita−Baylis−Hillman reaction of a variety of conjugated nitroalkenes with activated nonenolizable carbonyl compounds such as glyoxylate,
trifluoropyruvate, pyruvaldehyde, and ninhydrin in the presence of 40−100 mol % of DMAP in acetonitrile or 100 mol % of imidazole in CHCl3
or THF provided the adducts in decent to good yields. In most cases, the reactions catalyzed by DMAP in acetonitrile were faster and provided
the desired MBH adducts in higher yields as compared to the imidazole catalyzed reactions.
创建时间：
2016-05-05
