A New Approach to Nitrones through Cascade Reaction of Nitro Compounds Enabled by Visible Light Photoredox Catalysis
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https://figshare.com/articles/dataset/A_New_Approach_to_Nitrones_through_Cascade_Reaction_of_Nitro_Compounds_Enabled_by_Visible_Light_Photoredox_Catalysis/2207260
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资源简介：
A series of nitroalkanes
were efficiently transformed to alkylnitrones
using a visible light irradiation photocatalytic process. The mild,
efficient, and environmentally benign reaction method, involving dynamic
reciprocations of cascade pathways, comprises a mixture of a Ru(bpy)3Cl2 photoredox catalyst and DIPIBA or Hünig’s
base in CH3CN. Notably, DIPIBA was found to be the best
additive for the cross condensation reaction of nitroalkanes with
aldehydes. The structures of appropriate products were confirmed by
X-ray analysis.
创建时间：
2015-05-15
