CuI Mediated One-Pot Cycloacetalization/Ketalization of o‑Carbonyl Allylbenzenes: Synthesis of Benzobicyclo[3.2.1]octane Core
收藏Figshare2017-03-23 更新2026-04-29 收录
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https://figshare.com/articles/dataset/CuI_Mediated_One-Pot_Cycloacetalization_Ketalization_of_i_o_i_Carbonyl_Allylbenzenes_Synthesis_of_Benzo_bicyclo_3_2_1_octane_Core/4781131
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资源简介：
CuI/DMSO-mediated intramolecular cycloacetalization/ketalization of o-carbonyl allylbenzenes has been achieved for constructing [6,6,5]-tricycles having a ketal motif in good yields. The expeditious one-step route provides a three C–O bond formation. The key products with the structural framework of a benzofused dioxabicyclo[3.2.1]octane core have been confirmed by X-ray crystallographic analysis. Synthesis of dihydroisocoumarin has been studied.
创建时间：
2017-03-23
