The role of the copper surface in mechanocatalysis: A case study on mechanochemical sulfonylurea synthesis

This dataset contains raw NMR, XPS, ICP-MS, and DFT supporting our investigation of the role of the copper surface in the direct mechanocatalytic synthesis of tolbutamide. In addition to this data, a Microsoft Excel spreadsheet organizing the reactions run, amounts of reagents used, and conversions measured along with files for data processing and analysis are provided.