Overview of the data obtained from the ESI-negative FT-ICR-MS analysis.

The number of masses detected in all biological triplicates of each time point is shown. The data refer to the dataset obtained after applying the filtration criteria described in the Materials and Methods section. Values in brackets represent the percentages of masses to which a unique molecular formula could be assigned and the percentages of unique molecular formula containing heteroatoms. Isotopologues of assigned molecular formulae are not counted as assigned. Overall, a unique molecular formula could be assigned to 4,122 masses, corresponding to 49% of the obtained m/z.