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The morphology of vanadate glasses containing BaTiO3

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The morphology of vanadate glasses doped with BaTiO3 was measured. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated (573 K) brass plate and pressed by another plate.  An Olympus LEXT OLS4000 confocal scanning laser microscope (CSLM, Olympus Life Science, Hambur, Germany ) was used to examine the morphology of as-quenched surfaces and polished surfaces of samples. 3D color images were obtained using a 405 nm laser and photomultiplier detector with the maximum obtained optical magnification of 2160x. Detailed information can be found in: http://dx.doi.org/10.1016/j.jnoncrysol.2014.01.008
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Natalia Anna Wójcik
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