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A look inside a flexible open-source scanning electrochemical probe microscope

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DataONE2025-12-12 更新2025-12-20 收录
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Scanning electrochemical probe microscopy (SEPM) maps and investigates the chemical and physical properties of surfaces and interfaces using a micro- or nanoscale electrochemical probe, e.g., a microelectrode or a nanopipette, positioned close to an interface of interest. SEPMs share a common general architecture but are distinct from each other through the choice of probe and in the different physicochemical properties of the sample that can be investigated, including, among others, interfacial charge transfer rates, topography, permeability, or surface charge. Thus, a single instrument, with an appropriately flexible control system, can facilitate widespread access to the family of SEPM techniques - scanning electrochemical microscopy (SECM), scanning ion conductance microscopy (SICM), scanning electrochemical cell microscopy (SECCM), the scanning micropipette contact method (SMCM), and hybrid varieties of these techniques. Herein, we describe in detail a flexible open-source SEPM ins..., , # Data from: A look inside a flexible open-source scanning electrochemical probe microscope Dataset DOI: [10.5061/dryad.9p8cz8wx3](https://doi.org/10.5061/dryad.9p8cz8wx3) ## Description of the data and file structure Comma-separated text file representing SICM imaging of topography and BH~4~^-^ electrooxidation on a Au nanocluster (AuNC) in 30 mM NaOH (pH 12.5) aqueous solution with 3 mM NaBH~4~. Figures and tables refer to the associated primary article. ### Files and variables * ScanHopping.tsv Columns represent: | Data Channel Name | Units | Description | Breakout Box Connector | | :---------------- | :----------------------- | :---------------------------------------------------------------------------------------------------------- | :--------------------- | | X | µm | Measured X Piezo Position ...,
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2025-12-13
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