Controlling the symmetry of perylene derivatives via selective Or-tho-Borylation: Raw data

<p>This work presents a systematic and rational approach to the synthesis of previously reported as well as novel tetra- and di- ortho-borylated perylene, perylenediimide, and perylenemonoimide scaffolds. Through optimization of reaction conditions, employing [Ir(OMe)(COD)]₂ as a catalyst and the suitable ligands, efficient tetraborylation and regioselective diborylations were achieved. Additionally, the reaction times were reduced from days to hours under microwave irradiation, rendering this methodology a practical and scalable route for the ortho-functionalization of perylene derivatives.</p>

<p>The dataset contains the raw data in pdf of the High resolution Mass Spectrometry measurements as well as the original files provided by the UV-Vis absorption and fluorescence apparatus. </p>